Mass standards
Calibration range
The normal mass calibration range is from 1 mg to 50 kg. Uncertainties of measurement range from 40 parts in 109 at 1 kg to 2 parts in 107 at 50 kg. Calibration at routine higher uncertainties should be arranged through laboratories accredited by the Standards Council of Canada and NRC's Calibration Laboratory Assessment Service. A list of these laboratories is available. Sets of weights typically range from 1 mg to 100 g. They are calibrated by closed orthogonal designs using NRC standards.
The results of all mass calibrations normally represent conventional mass, i.e., the mass an artifact would appear to possess at an air density of 1.2 kg/m3. All uncertainties are expressed so as to relate the calibrated mass value to that of the international prototype of the kilogram. Absolute masses (the mass that a weight would appear to have a vacuum) are also determined when the densities are known.
Uncertainties on the order of 2 parts in 106 or better require a separate determination of density. This information can either be supplied by the client or established by NRC as a separate procedure. NRC will be the sole arbiter of acceptability of any density estimate from an external source. NRC does not calibrate, repair or certify balances or comparators.
Uncertainties
The uncertainties quoted in the descriptions below are expanded uncertainties representing a confidence level of approximately 95 percent, except where otherwise indicated. They were obtained assuming a normal distribution and multiplying the standard uncertainty (one standard deviation) by a coverage factor of k=2.
Fees for service
If you wish to order a calibration service, please request a quote from the following technical contact:
Dr. Claude Jacques
Telephone: 613-993-9330
Email: Claude.Jacques@nrc-cnrc.gc.ca
Note that the calibration costs quoted DO NOT include shipping, insurance or the cost of a customs broker. The client must arrange and pay for these services separately.
| Calibration number | Description | Fee |
|---|---|---|
| A33-05-00-00 | Custom mass standards measurements or services | Fee on request |
| A33-05-00-01 | Handling fee. A charge is levied for any instrument or artifact found to be unsuitable for calibration. This fee covers opening, inspection and return and is based on the work done prior to discovery of the fault. | $ 250 |
Mass
| Calibration number | Description | Fee |
|---|---|---|
| A33-05-01-00 | Setup. Set up for services A33-05-01**, applies to all. | $ 600 |
| A33-05-01-01a | Single weights. For weights up to 10 kg. Manual comparator. The charge for A33-05-01-00 also applies. | $ 200 |
| A33-05-01-01b | Single weight. For weights up to 10 kg. Automatic comparator. The charge for A33-05-01-00 also applies. | $ 250 |
| A33-05-01-01c | Single weight > 10 kg. The charge for A33-05-01-00 also applies. | $ 320 |
| A33-05-01-03 | Loading weights for dead weight gauges. Calibration of loading weights for dead weight gauges is carried out directly traceable to national standards, with an uncertainty of 1 part in 104. The charge for A33-05-01-00 also applies. | $ 110 |
| A33-05-01-06 | Reference weights - mass. Reference kilograms of adequate quality are compared with NRC primary stainless steel reference standards, using the NRC primary kilograms comparator. Conventional corrections are supplied with an uncertainty of 40 µg (40 ppb). The charge for A33-05-01-00 also applies. | $ 820 |
| A33-05-01-08 | Reference weights, comprehensive. Includes mass calibration as per A33-05-01-06 plus determinations of density, height of centre of mass, and magnetic susceptibility. The variation of the height of the centre of mass can effectively alter the apparent mass of the 1 kg weight by 3 µg to 5 µg. High magnetic susceptibility renders a weight unfit for calibration. The charge for A33-05-01-00 also applies. | $ 1,650 |
| A33-05-01-10 | Weight set orthogonal. The charge for A33-05-01-00 also applies. | $ 3,355 |
| A33-05-01-11 | Weight set orthogonal. The charge for A33-05-01-00 also applies. | $ 606 |
| A33-05-01-20 | Centre of mass. Determination of the height of the centre of mass of a kg reference weight. See A33-05-01-08. The charge for A33-05-01-00 also applies. | $ 370 |
Magnetic susceptibility of weights
The accuracy of mass measurement can be greatly affected by the magnetic susceptibility of weights. For high accuracy and conformance to a class (E1 to E2 and some ASTM classes), it is important to verify that magnetic susceptibility is sufficiently small.
| Calibration number | Description | Fee |
|---|---|---|
| A33-05-01-30 | Disc samples. Determination of magnetic susceptibility of a disc sample greater than 30 mm in diameter. The charge for A33-05-01-00 also applies. | $ 370 |
| A33-05-01-32 | Additional disc sample. As per A33-05-01-30, for each additional disc sample of the same dimensions when supplied at the same time. The charge for A33-05-01-00 also applies. | $ 160 |
| A33-05-01-34 | Light weights. Determination of magnetic susceptibility of an OIML- or ASTM- shaped weight (50 g to 2 kg). The charge for A33-05-01-00 also applies. | $ 370 |
| A33-05-01-36 | Additional light weight. As per A33-05-01-34, for each additional weight of the same dimensions when supplied at the same time. The charge for A33-05-01-00 also applies. | $ 160 |
| A33-05-01-38 | Heavy weight. Determination of magnetic susceptibility of an OIML- or ASTM- shaped weight (3 kg to 10 kg). The charge for A33-05-01-00 also applies. | $ 370 |
| A33-05-01-40 | Additional heavy weight. As per A33-05-01-38, for each additional weight of the same dimensions when supplied at the same time. The charge for A33-05-01-00 also applies. | $ 220 |
Hydrometers, density and volume
The derived quantity of density is generally measured in terms of the water or silicon standards. The densities of liquids and solids, particularly weights, are determined. Precision pycnometers are calibrated traceable to primary base SI quantities. Air densities are routinely computed and are used in aerostatic density measurements, when necessary. Results are based on calculations made at 20 °C unless otherwise requested by the client.
NRC calibrates sensitive hydrometers graduated in any type of unit. Each hydrometer must have a serial number and be made of either glass or metal. Hydrometers in the density range of 475 kg/m3 to 1800 kg/m3 are calibrated with an uncertainty of 1 part in 103, depending on the quality of the hydrometer. Calibrations are carried out by hydrostatic weighing in doubly distilled de-ionized water. If the hydrometer reading is affected by the surface tension of the liquid into which it is placed, the applicable surface tension value must be specified.
| Calibration number | Description | Fee |
|---|---|---|
| A33-05-02-00 | Setup. Preparation and installation of a batch for calibrations. This charge applies to every batch of services A33-05-02-01, A33-05-02-03, A33-05-02-04, A33-05-02-05. | $ 600 |
| A33-05-02-01 | Hydrometers. Calibration of one hydrometer at 3 measurement points. The charge for service A33-05-02-00 also applies. | $ 285 |
| A33-05-02-03 | Densities of weights. Densities of weights in the range of 7 500 kg/m3 to 17 000 kg/m3 with masses of 10 g to 1 kg are determined hydrostatically with an uncertainty of two parts in 103. The densities are traceable to the water density standard and the national prototype of the kilogram. Lower levels of uncertainty may be obtained by special arrangement. The charge for service A33-05-02-00 also applies. | $ 575 |
| A33-05-02-04 | Densities of liquids 600 kg/m3 - 2 000 kg/m3. Densities of liquids in the range of 600 kg/m3 to 2000 kg/m3 are determined by hydrostatic weighing using de-ionized doubly distilled water as a density standard and fused silica artifacts as solid transfer standards. Samples must be clearly marked. Special arrangements must be made for samples that are corrosive, volatile at ambient temperatures, toxic or very viscous. Solutions of thallium compounds are not accepted for calibration. The charge for service A33-05-02-00 also applies. | $ 400 |
| A33-05-02-05 | Densities of liquids in the range of 1 000 kg/m3 to 1 800 kg/m3. Densities of liquids in the range of 1 000 kg/m3 to 1 800 kg/m3 are determined as in A33-05-02-04 or gravimetrically using pure water as a reference standard by means of calibrated pycnometers. The charge for service A33-05-02-00 also applies. | $ 624 |
| A33-05-02-06 | Determinations of volume. Determination of the volume of volumetric glassware, pycnometers, constant volume delivery devices, syringes and other devices is performed gravimetrically. Due to the variety of such devices and the range of complexity in their volumetric calibration, this work is undertaken only by special arrangement. | Fee on request |
Pressure
The primary pressure standard is embodied in a mercury manometer that serves as the means of realization of the derived SI unit of pressure, the pascal (Pa). Dead weight piston gauges, also known as piston gauges, piston-cylinder gauges or pressure balances, provide traceable overlapping standards to higher pressures.
Preparation and shipping
Clients should refer to "Ordering calibration services" in the ÈCalibration services" pages for general information about shipping. In addition, the following points should be observed when sending pressure balances to NRC for calibration.
- It is generally unnecessary to ship the frame of the device.
- Separate the piston from the cylinder and clean both thoroughly, using warm soapy water. Rinse well and finish cleaning using 95 percent reagent grade ethanol or isopropanol.
- Pack the piston and cylinder carefully and separately in their own container or containers. This is particularly important when they are shipped with the loading weights.
- If the piston and weight carrier can be separated, be sure that the carrier is included in the shipment. NRC personnel will not attempt to separate seized assemblies that appear to have an interference fit.
Pneumatic pressure calibrations
| Calibration number | Description | Fee |
|---|---|---|
| A33-05-03-01 | Dead weight gauges, medium accuracy. Routine evaluation of the areas of dead weight assemblies (piston-cylinder assemblies) are carried out, with uncertainties > 0.01 percent, by comparisons with reference dead weight gauges traceable to the primary mercury manometer. | $ 1,600 |
| A33-05-03-01A | Dead weight gauges, high accuracy. Routine evaluation of the areas of dead weight assemblies (piston-cylinder assemblies) are carried out, with uncertainties < 0.01 percent, by comparisons with reference dead weight gauges traceable to the primary mercury manometer. | $ 3,150 |
| A33-05-03-06 | Pneumatic pressure gauges. Vibrating cylinder gauges, quartz bourdon gauges, liquid-in-glass manometers, and barometers and micromanometers are calibrated with an uncertainty of 0.01 percent. | $ 2,100 |
Hydraulic pressure calibrations
High pressure calibration is performed in the range from 200 kPa to 280 MPa using either a primary pressure balance or a reference dead weight standard with the indicated uncertainties. Zero and general stability tests, linearity tests, and points in excess of 10 required can be done for an additional fee. Please inquire directly about these and other special calibration requirements.
| Calibration number | Description | Fee |
|---|---|---|
| A33-05-03-21 | Hydraulic pressure gauges.Vibrating cylinder gauges, quartz bourdon gauges, etc., are calibrated with an uncertainty of 0.01 percent using reference dead weight tester. | $ 2,150 |
| A33-05-03-22 | Dial Gauges. Bourdon type gauges are calibrated using reference dead weight testers. Calibration uncertainty depends upon the gauge being calibrated. | $ 780 |
| A33-05-03-23 | Dead weight gauges < 100 MPa.Routine evaluation of the areas of piston-cylinder assemblies are carried out, with uncertainties < 0.01 percent by comparisons with reference dead weight gauges traceable to the primary mercury manometer. | $ 3,100 |
| A33-05-03-24 | Dead Weight Gauges > 100 MPa. Routine evaluation of the areas of piston-cylinder assemblies are carried out, with uncertainties > 0.01 percent by comparisons with reference dead weight gauges traceable to the primary mercury manometer. | $ 1,560 |
Flow (gas)
Gas flow is measured using a volume displacement apparatus using air or inert reference gases, such as nitrogen or argon. Because of the nonlinearity of flow devices, ten calibration points are recommended over the useful range of an instrument.
| Calibration number | Description | Fee |
|---|---|---|
| A33-05-05-01 | Gas flow gauge - set up charge.Set up for services A33-05-05-02. | $ 740 |
| A33-05-05-02 | Gas flow gauge - calibration.Gas flow gauges are calibrated for flows of 1 ml per minute to 50 standard litres per minute, with an uncertainty of 2 percent. The charge for service A33-05-05-01 also applies. | $ 130 per point |
Contact
Dr. Claude Jacques
Telephone: 613-993-9330
Email: Claude.Jacques@nrc-cnrc.gc.ca
Business Office: inmsbusino@nrc-cnrc.gc.ca
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